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2 article(s) from García-Verdugo, Eduardo

Synergy between supported ionic liquid-like phases and immobilized palladium N-heterocyclic carbene–phosphine complexes for the Negishi reaction under flow conditions

Edgar Peris,
Raúl Porcar,
María Macia,
Jesús Alcázar,
Eduardo García-Verdugo and
Santiago V. Luis

Beilstein J. Org. Chem. 2020, 16, 1924–1935, doi:10.3762/bjoc.16.159

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Graphical Abstract

Scheme 1: Synthesis of NHC-supported catalysts.

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Scheme 2: Negishi benchmark reaction.

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Figure 1: Negishi reaction catalyzed by immobilized NHC–Pd complexes. Conditions: methyl 4-bromobenzoate (0.2...

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Scheme 3: Synthesis of immobilized NHC–Pd–RuPhos.

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Figure 2: Negishi model reaction between 5 and 6 under flow conditions catalyzed by 4b. V = 0.535 mL, 363 mg ...

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Figure 3: Negishi model reaction under flow conditions catalyzed by 8a. V = 2.9 mL, 1.25 g of catalyst, resid...

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Figure 4: Negishi reaction between 5 and 6 catalyzed by 8a in the presence of SILLPs. a) Yield (%) vs time fo...

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Figure 5: TEM images of the polymers after the Negishi reaction between 5 and 6. a) 8a, bar scale 20 nm, PdNP...

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Scheme 4: Pd species immobilized onto SILLPs. i) 1 g SILLP 10, 100 mg PdCl₂ in milli-Q^® water (100 mL 1% HCl,...

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Figure 6: Negishi reaction between 5 and 6 catalyzed by 11. 1 equiv methyl 4-bromobenzoate (6, 0.25 mmol), 2 ...

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Figure 7: Negishi reaction between 5 and 6 under flow conditions catalyzed by 8a in the presence of a scaveng...

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Figure 8: Effect of the structure of the SILLP scavenger for the Negishi reaction between 5 and 6 under flow ...

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Figure 9: TEM images of the polymer after the Negishi reaction between 5 and 6 under flow conditions. a) 8a + ...

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Supp Info

Full Research Paper

Published 06 Aug 2020

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Efficient and selective chemical transformations under flow conditions: The combination of supported catalysts and supercritical fluids

M. Isabel Burguete,
Eduardo García-Verdugo and
Santiago V. Luis

Beilstein J. Org. Chem. 2011, 7, 1347–1359, doi:10.3762/bjoc.7.159

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Scheme 1: Hydrogenation of ethyl pyruvate.

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Scheme 2: Hydrogenation of dimethyl itaconate.

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Scheme 3: a) Enantioselective hydrogenation of N-(1-phenylethylidene)aniline in IL–CO₂; b) Enantioselective h...

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Scheme 4: Selective hydroformylation with a silica supported Rh catalyst.

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Scheme 5: Enantioselective hydroformylation of styrene.

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Scheme 6: Enantioselective hydrovinylation of styrene.

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Scheme 7: Enantioselective cyclopropanation of styrene catalyzed by supported Cu–BOX, Cu–PyOX and Rh–PyBOX ca...

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Scheme 8: Continuous hydrogenation of acetophenone coupled with the kinetic resolution of the product.

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Scheme 9: Kinetic resolution of phenylethanol using CALB immobilized in ILs and supported ILs.

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Review

Published 30 Sep 2011

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